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2006, ISBN: 9780471749448

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Wiley-Interscience, Gebundene Ausgabe, Auflage: 2. 384 Seiten, Publiziert: 2006-06-13T00:00:01Z, Produktgruppe: Buch, 1.45 kg, Verkaufsrang: 4805, Chemie, Naturwissenschaften & Technik, K… Más…

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Kolb, Bruno, Ettre, Leslie S.:
Static Headspace-Gas Chromatography: Theory and Practice - encuadernado, tapa blanda

2006

ISBN: 9780471749448

Wiley-Interscience, Gebundene Ausgabe, Auflage: 2. 384 Seiten, Publiziert: 2006-06-13T00:00:01Z, Produktgruppe: Buch, 1.45 kg, Verkaufsrang: 4893, Chemie, Naturwissenschaften & Technik, K… Más…

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Kolb, Bruno, Ettre, Leslie S.:
Static Headspace-Gas Chromatography: Theory and Practice - encuadernado, tapa blanda

2006, ISBN: 9780471749448

Wiley-Interscience, Gebundene Ausgabe, Auflage: 2. 384 Seiten, Publiziert: 2006-06-13T00:00:01Z, Produktgruppe: Buch, 1.45 kg, Verkaufsrang: 4893, Chemie, Naturwissenschaften & Technik, K… Más…

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Kolb, Bruno, Ettre, Leslie S.:
Static Headspace-Gas Chromatography: Theory and Practice - encuadernado, tapa blanda

2006, ISBN: 9780471749448

Wiley-Interscience, Gebundene Ausgabe, Auflage: 2. 384 Seiten, Publiziert: 2006-06-13T00:00:01Z, Produktgruppe: Buch, 1.45 kg, Verkaufsrang: 4805, Chemie, Naturwissenschaften & Technik, K… Más…

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Detalles del libro
Static Headspace-Gas Chromatography: Theory and Practice

The only reference to provide both current and thorough coverage of this important analytical technique Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC. Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover: * Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC * Basic theory of headspace analysis-physicochemical relationships, sensitivity, and the principles of multiple headspace extraction * HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques * Sample handling * Cryogenic HS-GC * Method development in HS-GC * Nonequilibrium static headspace analysis * Determination of physicochemical functions such as vapor pressures, activity coefficients, and more Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.

Detalles del libro - Static Headspace-Gas Chromatography: Theory and Practice


EAN (ISBN-13): 9780471749448
ISBN (ISBN-10): 0471749443
Tapa dura
Año de publicación: 2006
Editorial: Wiley-Interscience
349 Páginas
Peso: 0,635 kg
Idioma: eng/Englisch

Libro en la base de datos desde 2007-05-29T05:02:35-05:00 (Mexico City)
Página de detalles modificada por última vez el 2023-11-30T04:33:37-06:00 (Mexico City)
ISBN/EAN: 0471749443

ISBN - escritura alterna:
0-471-74944-3, 978-0-471-74944-8
Mode alterno de escritura y términos de búsqueda relacionados:
Autor del libro: kolb, bruno, ettre, leslie
Título del libro: rom, static, chromatography, sorry out gas, headspace, theory wants, the practice


Datos del la editorial

Autor: Bruno Kolb; Leslie S. Ettre
Título: Static Headspace-Gas Chromatography - Theory and Practice
Editorial: Wiley-Interscience; John Wiley & Sons
376 Páginas
Año de publicación: 2006-06-13
Peso: 0,630 kg
Idioma: Inglés
162,00 € (DE)
Not available (reason unspecified)
160mm x 238mm x 22mm

BB; Hardcover, Softcover / Chemie; Chromatographie; Chemie; Chemistry; Chromatographie / Trennverfahren; Chromatography / Separation Techniques; Gaschromatographie; Chromatographie / Trennverfahren

Preface. Preface to the First Edition. List of Acronyms and Symbols. 1. General introduction. 1.1 Principles of headspace analysis . 1.2 Types of headspace analysis. 1.3 The evolution of the HS-GC methods. 1.4 Headspace -- gas chromatography literature. 1.5 Regulatory methods utilizing (static) HS-GC. 1.6 References. 2. Theoretical background of HS-GC and its applications. 2.1 Basic theory of headspace analysis. 2.2 Basic physicochemical relationships. 2.3 Headspace sensitivity. 2.4 Headspace linearity. 2.5 Duplicate analyses. 2.6 Multiple headspace extraction (MHE). 2.7 References. 3. The technique of HS-GC. 3.1 Sample vials. 3.2 Caps. 3.3 Septa. 3.4 Thermostatting. 3.5 The fundamentals of headspace sampling systems. 3.6 Use of open-tubular (capillary) columns. 3.7 Enrichment techniques in HS-GC. 3.8 Special techniques with the balanced-pressure systems. 3.9. Reaction HS-GC. 3.10 References. 4. Sample handling in HS-GC. 4.1 Equilibration. 4.2 Solution approach. 4.3 Sample handling and sample introduction. 4.4 Preparation of standard solutions. 4.5 Influence of the matrix. 4.6 Methods aiming the complete evaporation of the analyte. 4.7 References. 5. Headspace methods for quantitative analysis. 5.1 Internal normalization. 5.2 Internal standard method. 5.3 External standard method. 5.4 Standard addition method. 5.5 Multiple headspace extraction (MHE). 5.6 Analysis of solid samples (adsorption systems). 5.7 Calibration techniques with headspace samples of varying volumes. 5.8 Analysis of gas samples. 5.9 References. 6. Method development in HS-GC. 6.1 General guidelines. 6.2 Determination of the residual monomer content of polystyrene pellets. 6.3 Determination of residual solvents in a printed plastic film. 6.4 Determination of the volatile constituents of a cathodic electrolytic plating bath. 7. Nonequilibrium static headspace analysis. 7.1 Accelerated analysis. 7.2 Heat-sensitive samples. 7.3 References. 8. Qualitative analysis by HS-GC. 8.1 The use of HS-GC in 'fingerprinting.'. 8.2 The use of headspace sampling in hyphenated systems. 8.3 The use of HS-GC in microbiology. 8.4 References. 9. Special measurements. 9.1 Determination of vapor pressures. 9.2 Determination of activity coefficients. 9.3 Determination of related physicochemical functions. 9.4 Determination of phase distribution (partition coefficient). 9.5 Reaction constant measurements. 9.6 Determination of solute solubility by MHE. 9.7 Gas-solid systems. 9.8 Validation of the headspace instrumentation: investigation of detector linearity and detection limit. 9.9 References. Index.

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